Sample 65501
65501 – 618 grams 65510 – 410 grams
Section titled “65501 – 618 grams 65510 – 410 grams”Soil and rake residue

Figure 1: Close-up photo of area where soil 65500 and rake sample 65510 were taken. AS16-107-17493


Figures 2 and 3: Maps of location of 65501 and 65510 at station 5 on Cayley Plain.

Figure 4: Composition of Apollo soil samples with that of 65501 shown.
Introduction
Section titled “Introduction”The astronauts stopped at Station 5 on the way back to the LM, where they collected several rake and soil samples at the base of Stone Mountain (figure 2). 65501 and 65510 contained a high proportion of soil clods (altogether there are 150 grams of soil clods in the rake sample 65510). These can be seen in figure 1.
Petrography
Section titled “Petrography”The maturity index for 65501 is low ( $I_s$ /FeO = 38). Butler et al. (1973) determined the grain size distribution (figure) and the modal mineralogy. The abundance of fragments of soil clods makes for an unusual distribution of grain size (figure 8) and a high value for the average grain size (149 microns).
Keil et al. (1972) and Warner et al. (1976) reported on rake samples from 65510. They were mostly soil clods (see figure 1).
Chemistry
Section titled “Chemistry”Baedecker et al. (1972), Duncan et al. (1973), Nava (1974), Philpotts et al. (1973) and Korotev (1982) all reported analyses of 65501 and 65510 (table 1).

Figure 5: The composition of 65501 is slightly less aluminous.

Figure 6: Carbon content and maturiy index for 65501 (Morris 1978; Moore et al. 1973).
Kerridge et al. (1975a) determined 90 ppm carbon and 60 ppm nitrogen for 65500 (figure 6), while Epstein and Taylor (1973) reported carbon (110 ppm), hydrogen and isotopic ratios for 65513(?). Kothari and Goel (1973) reported 80 ppm nitrogen.
Jovanovic and Reed (1973) determined the halogens, Li, U and Te. Cirlin and Housley (1981) determined the content of Cd (120 ppb) and Zn (22 ppm).


Figure 7: Normalized rare-earth-element diagram for 65501.
Other Studies
Section titled “Other Studies”Wieler et al. (1980) determined the density of fossil nuclear tracks.
Bogard and Nyquist (1973) and Walton et al. (1973) determined the rare gas content and isotopic ratios for 65501 and 65511.
Becker and Clayton (1977) calculated an exposure age of 510 m.y. from the abundance of 15N and compared this to the 310 m.y. 21Ne age of Walton et al. (1973).

average grain size = 149 microns

Figure 8: Grain size distribution for 65501 (Graf 1993, from data by Butler et al.).

Table 1. Chemical composition of 65501 and 65511.
| weight | reference Korotev82 | Baedecker72 Nava74 | 65500 | Philpotts73 < 570 um | Duncan73 Korotev81 | ave. st. 5 | 65511 Korotev82 | ||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| SiO2 % TiO2 Al2O3 FeO MnO MgO | 25.6 6.02 0.075 7 | (a) (a) (a) (a) | 46.2 0.62 25.17 5.65 0.072 6.91 | (e) (e) (e) (e) (e) (e) | 44.86 0.7 25.89 6.05 0.079 6.28 | (d) 45.3 (d) 0.65 (d) 26.2 (d) 5.85 (d) 0.075 (d) 6.25 | 25.3 5.82 0.08 6.7 | (a) (a) (a) (a) | |||||
| CaO Na2O K2O P2O5 S % sum | 14.2 0.473 | (a) (a) | 14.25 0.139 0.137 | (e) (e) | (e) 0.138 | 14.9 0.44 (c ) 0.148 0.157 0.082 | (d) (d) | (d) 15 (d) 0.45 (d) 0.134 | 14.2 0.474 | (a) (a) | |||
| Sc ppm V Cr Co Ni | 10.2 20 830 36.4 515 | (a) (a) (a) (a) | (a) 491 | (b) | 821 | (e) | 290 | 10.1 25 780 31 430 | 10.6 24 847 26.3 370 | (a) (a) (a) (a) (a) | |||
| Cu Zn Ga Ge ppb As Se | 26 5.6 1250 | (b) (b) (b) | 5.7 23 | ||||||||||
| Rb Sr Y | 155 | (a) | 3.56 162 | (c ) 3.84 (c ) 162 48 | (d) 3.3 (d) 162 (d) 48 | 165 | (a) | ||||||
| Zr Nb Mo Ru Rh Pd ppb Ag ppb | 215 | (a) | 228 15 | (d) | (d) 205 | 240 | (a) | ||||||
| Cd ppb In ppb Sn ppb Sb ppb Te ppb | 100 16 | (b) (b) | |||||||||||
| Cs ppm Ba | 0.16 175 | (a) (a) | 165 | (c ) 175 | (d) 130 | 0.17 172 | (a) (a) | ||||||
| La Ce Pr | 14.7 39.5 | (a) (a) | 37.6 | (c ) | 14.4 | 15.9 42.7 | (a) (a) | ||||||
| Nd Sm Eu | 7.03 1.211 | (a) (a) | 24.2 6.9 1.26 | (c ) (c ) (c ) | 6.7 1.24 | 7.56 1.233 | (a) (a) | ||||||
| Gd Tb | 1.49 | (a) | 8.63 | (c ) | 1.44 | 1.59 | (a) | ||||||
| Dy Ho | 9.12 | (c ) | |||||||||||
| Er Tm | 5.46 | (c ) | |||||||||||
| Yb Lu Hf Ta W ppb Re ppb Os ppb | 4.99 0.704 5.5 0.74 | (a) (a) (a) (a) | 5.02 0.768 | (c ) (c ) | 4.9 0.71 5.1 0.54 | 5.35 0.75 6.15 0.83 | (a) (a) (a) (a) | ||||||
| Ir ppb Pt ppb | 14.1 | (a) 14 | (b) | 10.5 | (a) | ||||||||
| Au ppb Th ppm U ppm | 2.77 0.7 | (a) (a) | 8.1 technique: (a) INAA, (b) RNAA, (c ) IDMS, (d) XRF, (e) AA | (b) | 2.2 0.67 | 2.84 0.74 | (a) (a) |
Lunar Sample Compendium C Meyer 2010
References for 65501.
Section titled “References for 65501.”Baedecker P.A., Chou C-L., Sunberg L.L. and Wasson J.T. (1972) Extralunar materials in Apollo 16 soils and the decay rate of the extralunar flux 4.0 GY ago. Earth Planet. Sci. Lett. 17, 79-83.
Becker R.H. and Clayton R.N. (1977) Nitrogen isotopes in lunar soils as a measure of cosmic-ray exposure and regolith history. Proc. 8th Lunar Sci. Conf. 3685-3704.
Bogard D.D. and Nyquist L.E. (1973) 40Ar/36Ar variations in Apollo 15 and 16 regolith. Proc. 4th Lunar Sci. Conf. 1975-1986.
Butler P. (1972) Lunar Sample Information Catalog Apollo 16. Lunar Receiving Laboratory. MSC 03210 Curator’s Catalog. pp. 370.
Butler J.C., Greene G.M. and King E.A. (1973) Grain size frequency distribution and modal analysis of Apollo 16 fines. Proc. 4th Lunar Sci. Conf. 267-278.
Cirlin E.H. and Housley R.M. (1981) Distribution and evolution of Zn, Cd, and Pb in Apollo 16 regolith samples and the average U-Pb ages of the parent rocks. Proc. 12th Lunar Planet. Sci. Conf. 529-540.
Duncan A.R., Erlank A.J., Willis J.P. and Ahrens L.H. (1973) Composition and inter-relationships of some Apollo 16 samples. Proc. 4th Lunar Sci. Conf. 1097-1113.
Epstein S. and Taylor H.P. (1973b) The isotopic composition and concentration of water, hydrogen, and carbon in some Apollo 15 and 16 soils and in the Apollo 17 orange soil. Proc. 4th Lunar Sci. Conf. 1559-1575.
Jovanovic S. and Reed G.W. (1973b) Volatile trace elements and the characterization of the Cayley formation and the primitive lunar crust. Proc. 4th Lunar Sci. Conf. 1313-1324.
Graf J.C. (1993) Lunar Soils Grain Size Catalog. NASA Pub. 1265
Keil K., Dowty E., Prinz M. and Bunch T.E. (1972) Description, classification and inventory of 151 Apollo 16 rake samples from the LM area and station 5. Curator’s Catalog, JSC.
Kerridge J.F., Kaplan I.R., Petrowski C. and Chang S. (1975) Light element geochemistry of Apollo 16 rocks and soils. Geochim. Cosmochim. Acta 39, 137-162.
Korotev R.L. (1982) Comparative geochemistry of Apollo 16 surface soils and samples from cores 64002 and 60002 thru 60007. Proc. 13th Lunar Planet. Sci. Conf. A269-A278. Kothari B.K. and Goel P.S. (1973) Nitrogen in lunar samples*. Proc. 4th Lunar Sci. Conf.* 1587-1596.
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Marvin U.B. (1972) Apollo 16 coarse fines (4-10 mm): Sample classification, description and inventory. JSC Catalog.
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Moore C.B. and Lewis C.F. (1975) Total nitrogen contents of Apollo 15, 16 and 17 lunar fines samples. Lunar Sci. VI, 569-571.
Morris R.V., Score R., Dardano C. and Heiken G. (1983) Handbook of Lunar Soils. Two Parts. JSC 19069. Curator’s Office, Houston
Morris R.V. (1978) The surface exposure (maturity) of lunar soils: Some concepts and Is/FeO compilation. Proc. 9th Lunar Sci. Conf. 2287-2297.
Nava D.F. (1974a) Chemical compositions of some soils and rock types from the Apollo 15, 16, and 17 lunar sites. Proc. 5th Lunar Sci. Conf. 1087-1096.
Philpotts J.A., Schumann S., Kouns C.W., Lum-Staab R.K.L. and Schnetzler C.C. (1973b) Apollo 16 returned lunar samples – lithophile trace-element abundances. Proc. 4th Lunar Sci. Conf. 1427-1436.
Sutton R.L. (1981) Documentation of Apollo 16 samples. In Geology of the Apollo 16 area, central lunar highlands. (Ulrich et al. ) U.S.G.S. Prof. Paper 1048.
Taylor H.P. and Epstein S. (1975) O18/O16 and Si30/Si28 studies of some Apollo 15, 16 and 17 samples. Proc. 4th Lunar Sci. Conf. 1657-1679.
Warner R.D., Dowty E., Prinz M., Conrad G.H., Nehru C.E. and Keil K. (1976c) Catalog of Apollo 16 rake samples from the LM area and station 5. Spec. Publ. #13, UNM Institute of Meteoritics, Albuquerque. 87 pp.
Wieler R., Etique Ph., Signer P. and Poupeau G. (1980) Record of the solar corpuscular radiation in minerals from lunar soils: A comparative study of noble gases and tracks. Proc. 11th Lunar Planet. Sci. Conf. 1369-1393.